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Beilstein J. Org. Chem. 2013, 9, 1668–1676, doi:10.3762/bjoc.9.191
Graphical Abstract
Figure 1: Formal, topological approach to derive coarctate reactions from pericyclic reactions; p, q: number ...
Figure 2: Stereochemistry of coarctate reactions derived from a Hückel (top) and a Möbius band (bottom). The ...
Scheme 1: Coarctate fragmentation of the spiroozonide derived from methylenecyclopropane.
Scheme 2: Photochemically and thermally allowed coarctate fragmentations of spiroketals.
Scheme 3: Precursors used in this study.
Figure 3: Difference infrared spectrum, showing the changes in the IR spectrum after photolysis (λexc = 254 n...
Figure 4: Infrared spectrum obtained upon FVP of 1 at T = 1143 K and trapping the pyrolysate in solid argon a...
Figure 5: Infrared spectrum obtained upon FVP of 2 at T = 963 K and trapping the pyrolysate in solid argon at ...
Figure 6: Infrared spectrum obtained upon FVP of 3 at T = 1043 K and trapping the pyrolysate in solid argon a...
Scheme 4: Possible fragmentation pathways in the FVP of 1.
Scheme 5: Possible fragmentation pathways in the FVP of 2.
Scheme 6: Possible fragmentation pathways in the FVP of 3.
Beilstein J. Org. Chem. 2013, 9, 613–614, doi:10.3762/bjoc.9.67